Exercises in Selected Processes of Chemical Industry

NAME OF THE COURSE Exercises in Selected Processes of Chemical Industry

Code

KTJ319

Year of study

3.

Course teacher

Prof Jelica Zelić

Credits (ECTS)

2.0

Associate teachers

Asst Prof Miće Jakić
Asst Prof Mario Nikola Mužek

Type of instruction (number of hours)

P S V T

0

0

30

0

Status of the course

Mandatory

Percentage of application of e-learning

0 %

COURSE DESCRIPTION

Course objectives

Qualifying students how to implement experiments in the laboratory and semi-industrial scale, and how to analysis the chemical and/or physical process in particular phases of technological processes of selected inorganic and organic industry.

Course enrolment requirements and entry competences required for the course

Enrolled in or passed the cours Selected Processes of Chemical Industry

Learning outcomes expected at the level of the course (4 to 10 learning outcomes)

After passing the course the student will be able to:
1. Conduct experiments in the laboratory and industry.
2. Perform measurements independently and teamwork.
3. Interpret the collected data and measurement results using the methodology of chemical engineering.
4. To analyze the chemical and / or physical processes according to present conditions and material properties.
5. Recommendation of process parameters in order to optimize processes in particular phases of production and application of selected inorganic and polymeric materials.

Course content broken down in detail by weekly class schedule (syllabus)

1. Water treatment. Water softening processes. Lime-Soda process. Ion-exchange process.
2. Electrochemical processes. Electrolysis of sodium chloride solution.
3. Catalytic processes. Contact oxidation of sulphur dioxide.
4. Hydration processes. Physical and chemical properties of silicate cement (density, specific surface area, normal consistency, sitting time, heat of hydration).
5. Chemical resistance of soda-lime-silica glass.
6. Physical and chemical properties of petroleum products (fuels and lubricants).
7. Dehydration of ethanol to acetaldehyde.
8. Esterification of phthalic anhydride with n-butanol (Synthesis of di-butyl phthalate).
9. Manufacture of soap.
10. Synthesis of azo dyes.
11. The sulphonation of styrene / divinyl benzene.
12. Step polymerization (synthesis of polyester or polyamide).
13. The radical chain polymerization (suspension polymerization of styrene emulsion polymerization of vinyl acetate).
For the proposed exercises pertaining to organic part of the student will make four (4).

Format of instruction:

Student responsibilities

Implementation and analysis of selected processes according to preset conditions.
Each student is required to do the entire exercises planned program. On completion of all exercises the final written exam is obligated.

Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course):

Class attendance

0.6

Research

0.0

Practical training

0.0

Experimental work

0.5

Report

0.4

 

 

Essay

0.0

Seminar essay

0.0

 

 

Tests

0.0

Oral exam

0.0

 

 

Written exam

0.5

Project

0.0

 

 

Grading and evaluating student work in class and at the final exam

Successful completion of laboratory works has share 60% and the final written exam 40% score. Exam passing score is 60%. Grades: 60% - 70% - satisfactory, 71% -81% - good, 82% -92% very good, and 93% -100% - excellent.

Required literature (available in the library and via other media)

Title

Number of copies in the library

Availability via other media

J. Zelić, Praktikum iz procesa anorganske industrije, Kemijsko-tehnološki fakultet u Splitu, Split, 2013. (recenzirani i objavljeni nastavni materijali)

1

www.ktf-split.hr

I. Klarić, Vježbe iz polimerizacije (za internu upotrebu), Tehnološki fakultet u Splitu, Split, 1990.

10

I. Klarić, Vježbe iz tehnoloških procesa organske industrije (za internu upotrebu), Tehnološki fakultet u Splitu, Split, 1990.

10

Optional literature (at the time of submission of study programme proposal)

R. Krstulović, Tehnološki procesi anorganske industrije, Sveučilišni udžbenik, Sveučilište u Splitu, Split, 1986.

Quality assurance methods that ensure the acquisition of exit competences

Quality of the teaching and learning monitored at the level of the
(1) teachers, accepting suggestions of students and colleagues, and
(2) Faculty, conducting surveys of students on teaching quality.

Other (as the proposer wishes to add)