Exercises in Process of Precipitation and Crystallization

NAME OF THE COURSE Exercises in Process of Precipitation and Crystallization

Code

KTA322

Year of study

3.

Course teacher

Assoc Prof Dražan Jozić

Credits (ECTS)

1.0

Associate teachers

Type of instruction (number of hours)

P S V T

0

0

15

0

Status of the course

Elective

Percentage of application of e-learning

0 %

COURSE DESCRIPTION

Course objectives

Students acquire the basics of the different crystalline states and their arrangements as well as the fundamentals of the processes of nucleation, precipitation and crystallization under different experimental conditions (water solution and melts).

Course enrolment requirements and entry competences required for the course

Enrolled in or passed the course Process of Precipitation and Crystallization

Learning outcomes expected at the level of the course (4 to 10 learning outcomes)

After passing the exam the student will be able to:
- Able to choose on the base of the physical and chemical properties suitable solvent
- Can choose a suitable precipitant agent for providing the process of precipitation
- Know the basic methods and procedures of dissolutions, precipitation and crystallization
- Known procedures and methods of recrystallization and purification of the product
- Basic knowledge about the industrial equipment for the crystallization process

Course content broken down in detail by weekly class schedule (syllabus)

1. Exercise. The processes of dissolution of inorganic salts.
2. Exercise. Funding for the precipitation and separation.
3. Exercise. Deposition processes in heterogeneous reaction systems.
4. Exercise. Separation and removal of salt.
5. Exercise. Crystallization from the melt.
6. Exercise. Crystallization from the gaseous phase.

Format of instruction:

Student responsibilities

Class attendance at the lecture in the amount of 70% to 100%, and to experimental work of 100% from total hours.

Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course):

Class attendance

0.0

Research

0.0

Practical training

0.0

Experimental work

0.5

Report

0.2

 

 

Essay

0.0

Seminar essay

0.0

 

 

Tests

0.3

Oral exam

0.0

 

 

Written exam

0.0

Project

0.0

 

 

Grading and evaluating student work in class and at the final exam

Selected articles from journals recommended by lecturer

Required literature (available in the library and via other media)

Title

Number of copies in the library

Availability via other media

Perry’s Chemical Engineers’ Handbook Seventh Edition, The McGraw-Hill Companies, Inc., New York, 1997.

0

A. Mersmann, Crystallization tchnology handbook, Marcell Dekker, New York, 2001.

0

Optional literature (at the time of submission of study programme proposal)

Selected articles from journals recommended by lecturer

Quality assurance methods that ensure the acquisition of exit competences

Tracking suggestions and reactions of students throughout the semester
Student survey

Other (as the proposer wishes to add)