| NAME OF THE COURSE |
Analytical chemistry |
|---|
Code |
|
Course teacher |
Prof Josipa Giljanović |
Credits (ECTS) |
8.0 |
|
Associate teachers |
Assoc Prof Ante Prkić |
Type of instruction (number of hours) |
|
|
Status of the course |
Mandatory |
Percentage of application of e-learning |
0 % |
|
| COURSE DESCRIPTION |
Course objectives |
Acquiring basic basic theoretical knowledge of analytical chemistry, the role and application of analytical chemistry in various fields |
Course enrolment requirements and entry competences required for the course |
Completing the course: General chemistry |
Learning outcomes expected at the level of the course (4 to 10 learning outcomes) |
After completing the course, the student will will be able to
- Define the concept of analytical chemistry
- Differentiate between the concepts of qualitative and quantitative chemical analysis
- Understand the concept of quantitative chemical reactions
- Understand the concept of gravimetric and volumetric determination
- Understand the precipitation, neutralization, complexometric and redox titrations
- Solving numerical problems from a qualitative and quantitative chemical analysis |
Course content broken down in detail by weekly class schedule (syllabus) |
First week : Description and review of curriculum. Definitions of analytical chemistry. Division of Analytical Chemistry. The concept of the analytical signal. Seminar: Solving numerical problems from theoretical lecture
Second week : The concept and definition of chemical analysis - qualitative and quantitative. Seminar: Solving numerical problems; homogeneous and heterogeneous equilibrium in analytical chemistry..
3rd week : Qualitative chemical analysis. The concept and definition of acids and bases. Consideration of acid-base balance. Seminar: Solving problems
.4th week : The concept and definition of complex ions., complexometric equilibrium . Seminar: Solving problems
5th week : The concept and definition of electrochemical reactions. Consideration of electrochemical equilibrium. Seminar: Solving problems
6th week: The concept and definition of heterogeneous equilibrium. process of dissolution and precipitation. Seminar: Solving problemsl
7th week .Recapitulation of theoretical and seminars lecture I partial exam .theoretical lecture and seminars
8th week . Quantitative chemical analysis. The concept and definition of gravimetric determination. Seminar: Solving problems,
9th week . Optimization of precipitationcondition. Seminar: Solving problems.
10th week : The concept and definition of standards and standard solutions - primary and secondary. The concept and definition of the volumetric determination; Seminar: Solving problems.
11th week : The concept and definition of volumetric determinations- Argentometric titration; Seminar: Solving problems.
12th weeks The concept and definition of volumetric determinations based on neutralization reactions - acid-base titration; Seminar Solving problems
13th week . The concept and definition of volumetric determinations based on the complex - complexometric titrations; Seminar Solving problems
14th week . The concept and definition of volumetric determinations based on redox reactions. Seminar Seminar Solving problems
15th week : Recapitulation of theoretical and seminars lecture II partial exam .theoretical lecture and seminars.
Laboratory excersise: Introduction to laboratory work. Qualitative chemical analysis – determination of group of cations and anions. Gravimetric determination nickel cations.
volumetric methods: Preparation of standard solutions. Acid-base titration.
Complexometric Titrations. Oxidation-reduction titration. Potentiometric titration |
Format of instruction: |
|
Student responsibilities |
Lectures attendance - at least 80% and completing exercises |
Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course): |
Class attendance |
1.0 |
Research |
0.0 |
Practical training |
0.0 |
Experimental work |
0.0 |
Report |
0.0 |
|
2.0 |
Essay |
0.0 |
Seminar essay |
0.0 |
|
|
Tests |
1.0 |
Oral exam |
2.0 |
|
|
Written exam |
2.0 |
Project |
0.0 |
|
|
|
Grading and evaluating student work in class and at the final exam |
The entire test can be applied over two partial tests during the semester. Passing threshold is 60%. Each test in assessing participates with 50%. Lectures presence of 80 to 100% is 10% marks. The examination periods there is a written and oral exam. Passing threshold is 60%. Passing one partial test of any part (previous activity) is valid throughout current academic year. Written exam has a share of 50% and oral examination also 50%. Students who have not passed the partial tests will have oral examination in the regular examination period. Passing threshold is 60% and the examination form to participate in the evaluation by 50%.
Rating: 60% -69% - satisfactory, 70% -79% - good, 80% -89% very good, 90% -100% - excellent. |
Required literature (available in the library and via other media) |
Title |
Number of copies in the library |
Availability via other media |
D. A. Skoog, D. M. West i F. J. Holler, Osnove analitičke kemije, Školska knjiga, Zagreb, 1999. |
6 |
|
A. Prkić, Vježbe iz analitičke kemije, Preddiplomski studij kemijske tehnologije, interna recenzirana skripta, Split, 2008. |
0 |
Web stranice KTF-a |
R. Kellner, J.M. Mermet, M. Otto, M. Varcarcel, H.M. Widmer, Analytical Chemistry (A Modern Approach to Analytical Science, 2nd Edition) Wiley-VCHVerlag Gmbh&Co. KGaA, Weinheim, 2004. |
0 |
|
D. A. Skoog, D. M. West i F. J. Holler, S. R. Crouch, Fundamentals of Analytical Chemistry, 9th edition, Brooks&Cole, SAD, 2014. |
0 |
|
|
Optional literature (at the time of submission of study programme proposal) |
Z. Šoljić, Računanje u analitičkoj kemiji, Zagreb, 1998.
|
Quality assurance methods that ensure the acquisition of exit competences |
- monitoring of students suggestions and reactions during semester
- students evaluation organized by University |
Other (as the proposer wishes to add) |
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