Selected processes of chemical industry

NAME OF THE COURSE Selected processes of chemical industry

Code

KTG311

Year of study

3.

Course teacher

Prof Jelica Zelić

Credits (ECTS)

5.5

Associate teachers

Asst Prof Miće Jakić

Type of instruction (number of hours)

P S V T

45

15

0

0

Status of the course

Mandatory

Percentage of application of e-learning

0 %

COURSE DESCRIPTION

Course objectives

Qualifying students for the adoption and application of the fundamental principles of chemical processes in technological processes of inorganic and organic industry with special emphasis on techno-economic and environmental aspects.

Course enrolment requirements and entry competences required for the course

Enrolled in or passed the course Selected processes of chemical industry- laboratory

Learning outcomes expected at the level of the course (4 to 10 learning outcomes)

After passing the course the student will be able to:
1. Classify and apply the basic principles of chemical processes in technological processes of inorganic and organic industry.
2. To explain the process and apply methods for the preparation of process water.
3. Categorize energy sources for inorganic processes and describe the processes of combustion of solid fuels.
4. Describe catalytic processes and influential factors in production processes basic inorganic chemical industry (ammonia, sulfuric acid, nitric acid).
5. Explain the basic processes (hydration, sintering) and the influential factors in the production of ceramic materials.
6. Distinguish metallurgical, electrothermical and electrochemical processes in relation to the implementation of the process, equipment, quality assurance, the possibility of using secondary raw materials and by-products of inorganic processes.
7. Compute important parameters for the phases of the production process.
8. Explain the basic processes (primary and secondary) of the processing of petroleum.
9. Distinguish and explain processes for production of components for organic synthesis (alkanes, alkenes, acetylene, aromatic hydrocarbons, synthesis gas) from the petrochemical sources (natural gas, petroleum).
10. Describe technological processes in organic synthesis.
11. Explain the processes of polymerisation.

Course content broken down in detail by weekly class schedule (syllabus)

1st week: Introduction. Elementary principles of chemical processes.
2nd week: Water in the technological processes. The precipitation agents, ion exchangers and membranes in the waters-treatment process (basic processes and reactions, equipment and process control).
3rd week: Energy sources for inorganic processes. Fuels and burning processes of solid fuels. Gas generator.
4th week: The most important examples of catalytic processes of the basic inorganic chemical industry (synthesis of ammonia, production of nitric and sulphuric acids). The written knowledge tests (I Colloquium).
5th week: The high-temperatures reaction in the solid state and sintering processes in the production of ceramic materials.
6th week: Forming processes of dispersion systems with water. Clay-water system.
7th week: Hydration processes and hardening of mineral binders.
8th week: Metallurgical and electrothermical processes. Electrochemical industrial processes, electrolyses of aqueous solutions and melting salts. The written knowledge tests (II Colloquium).
9th week: Primary and secondary processes of the processing of petroleum.
10th week: Processes for production of components for organic synthesis (alkanes, alkenes, acetylene, aromatic hydrocarbons, synthesis gas) from the petrochemical sources (natural gas, petroleum).
11th week: Alternative (no conventional) methods for raw materials production for organic synthesis.
12th week: Technological processes in organic synthesis according the criteria of similar chemical reactions (thermodynamics and kinetics, catalysts). The written knowledge tests (III Colloquium).
13th week: The production of fine chemicals. The processes of hydrogenation and dehydrogenation, hydroformilation and oxidation reactions.
14th week: The production of fine chemicals. The processes of alkylation, esterification and nitration.
15th week: The production of fine chemicals. The processes of sulfonation and sulphating, hydrolysis and polymerisation. The written knowledge tests
(IV Colloquium).
SEMINARS:
During the semester are processed numerical examples (tasks) from lectures and the flow diagram presentation of selected technological processes (physical and chemical base processes, equipment and environmental impact), which together with lectures seems a whole.

Format of instruction:

Student responsibilities

 

Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course):

Class attendance

1.0

Research

0.0

Practical training

0.0

Experimental work

0.0

Report

0.0

 

 

Essay

0.0

Seminar essay

0.5

 

 

Tests

1.0

Oral exam

1.5

 

 

Written exam

1.5

Project

0.0

 

 

Grading and evaluating student work in class and at the final exam

A student can pass a part or the entire exam by taking four (4) partial tests during the semester, i.e., two (2) partial tests from the inorganic part, and two (2) partial tests from the organic part. Test passing score is 60%. Students who do not pass the partial exams have to take an exam in the regular examination periods. The exam consists of theoretical (oral) and written part. Exam passing score is 60%.
Grades depending on the test score: 60% - 70% - satisfactory, 71% -81% - good, 82% -92% very good, and 93% 100% - excellent.

Required literature (available in the library and via other media)

Title

Number of copies in the library

Availability via other media

R. Krstulović, Tehnološki procesi anorganske industrije, Sveučilišni udžbenik, Sveučilište u Splitu, Split, 1986.

5

J. Zelić, Praktikum iz procesa anorganske industrije, Kemijsko-tehnološki fakultet u Splitu, Split, 2013. (recenzirani i objavljeni nastavni materijali), http://www.ktf-split.hr/bib/nm/Procesi_anorganske_industrije.pdf

1

www.ktf-split.hr

Z. Janović, Polimerizacije i polimeri, Hrvatsko društvo kemijskih inženjera i tehnologa, Zagreb, 1997.

6

I. Klarić, Tehnološki procesi organske industrije (I. dio), Kemijsko-tehnološki fakultet u Splitu, Split, 2008., (recenzirani i objavljeni nastavni materijali), https://www.ktf-split.hr/index.php/nastavni-materijali-knjiznice/repozitorij-265?start=20

0

www.ktf-split.hr

Z. Janović, Naftni i petrokemijski procesi i proizvodi, Hrvatsko društvo za goriva i maziva, Zagreb, 2011.

15

Optional literature (at the time of submission of study programme proposal)

J. Zelić, Z. Osmanović, Čvrstoća i trajnost cementnih kompozita, Sveučilišni udžbenik, Sveučilište u Splitu, 2014., ISBN 978-953-7803-01-8.
Z. Osmanović, J. Zelić, Proizvodnja Portland-cementa, Univerzitetski udžbenik, Univerzitet u Tuzli, B&H, Tuzla, 2010., ISBN 978-9958-897-04-7.
http://www.knjiga.ba/proizvodnja_portlandj_cementa-k7412.html

Quality assurance methods that ensure the acquisition of exit competences

Quality of the teaching and learning monitored at the level of the
(1) teachers, accepting suggestions of students and colleagues, and
(2) Faculty, conducting surveys of students on teaching quality.

Other (as the proposer wishes to add)