Analysis of Real Samples

NAME OF THE COURSE

Code

KTG306

Year of study

Course teacher

Assoc Prof Ante Prkić

Credits (ECTS)

3.5

Associate teachers

Type of instruction (number of hours)

P	S	V	T
30	15	0	0

Status of the course

Mandatory

Percentage of application of e-learning

0 %

COURSE DESCRIPTION

Course objectives

- Provide students with the basics of sampling.
- Teach students solve practical problems of sampling of real sample
- Introduction of students to basic methods for assessing the composition and size fractions in the real sample.

Course enrolment requirements and entry competences required for the course

Enrolled in or passed the course Exercise of Analysis of real samples

Learning outcomes expected at the level of the course (4 to 10 learning outcomes)

Implementation of the sampling process as the initial step of each chemical analysis
Proper selection of the quantity of collected material, depending on the analyte and the available analytical methods and techniques
Link Auditors solve problems related to sampling using statistical methods with the available techniques and methods which can be carried out chemical analysis
Learning to use mathematical tools in solving mathematical problems related to sampling

Course content broken down in detail by weekly class schedule (syllabus)

Week 1: Significance analysis of real samples: raw materials, industrial products. The development and control processes. Seminar: Solving numerical examples treated theoretical material.
Week 2: Sampling of gases, liquids and solids. Seminar: Solving numerical examples from the sampling of gases, liquids and solids.
Week 3: Analytical separation. Preparation of samples for analysis. Seminar: Solving numerical problems in the theory of analytic separation.
Week 4: Decomposition and dissolution of samples. Seminar: Solving numerical examples treated theoretical material - Decomposition and dissolution of samples.
Week 5: Development of selected methods. The choice of methods of analysis. Seminar: Solving numerical examples treated theoretical material - Development of selected methods.
Week 6: Reporting and interpretation of analytical data. Seminar: Solving numerical examples treated theoretical material - Reporting and interpretation of analytical data.
Week 7: Revision of theoretical and seminar materials. Assessment (first partial test of theoretical and seminar materials).
Week 8: Determination of water. Moisture in solids and gases. Seminar: Solving numerical examples treated theoretical material - moisture in solids and gases.
Week 9: Methods for the analysis of materials: cement, minerals, alloys and metals, oil, water. Seminar: Solving numerical examples treated theoretical materials - Methods for analysis of materials.
10th week: Quality control. Tolerance. Seminar: Solving numerical examples treated theoretical material - Quality control and tolerance.
11th week: Reference Materials. Seminar: Solving numerical examples treated theoretical material - Reference Materials.
12 weeks: Sampling and sample preparation for analysis of plaster and cement. Seminar: Solving numerical examples treated theoretical materials - Sampling plaster and cement.
13th week: Separation and Analysis of Minerals. Seminar: Solving numerical examples treated theoretical material - Collection and analysis of minerals.
14th week: Separation and analysis: alloy. Seminar: Solving numerical examples treated theoretical material - Collection and analysis of alloys.
Week 15: Revision of theoretical and seminar materials. Examination (II. Partial test theoretical and seminar materials).

Format of instruction:

Student responsibilities

Attending lectures in the amount of 80% of the hourly rate.

Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course):

Class attendance	0.3	Research	0.0	Practical training	0.0
Experimental work	0.0	Report	0.0
Essay	0.0	Seminar essay	0.3
Tests	0.0	Oral exam	1.5
Written exam	1.5	Project	0.0

Grading and evaluating student work in class and at the final exam

The entire examination can be applied over the two partial test of theoretical and seminar materials during the semester. Passing threshold is 60%. Each colloquium in the assessment accounts for 50%. Lectures presence of 80 to 100% is 10% marks. The examination periods there is a written, oral and written and oral examination. Passing threshold is 60%. Passing one partial test from any part (previous activity) is valid throughout the current academic year. Written exam has a share of 30% of oral and written with 60% and 10% verbal. Students who did not pass the exam by the partial tests take the exam through written, oral and written-oral examination in the regular examination periods. Passing threshold is 60% and the examination form to participate in the assessment with 50%.
Rating: 60% -69% - satisfactory, 70% -79% - a good 80% -89% -very good, 90% -100% - excellent.

Required literature (available in the library and via other media)

Title	Number of copies in the library	Availability via other media
D. A. Skoog, D. M. West i F. J. Holler, Osnove analitičke kemije, Školska knjiga, Zagreb, 1999.	6
A. I. Vogel, A. Tekst-book quantitative inorganic analysis, Fifth Edition Longman, London, 1986.	0
R. Kellner, J.M. Mermet, M. Otto, M. Varcarcel, H.M. Widmer, Analytical Chemistry (A Modern Approach to Analytical Science, 2nd Edition) Wiley-VCHVerlag Gmbh&Co. KGaA, Weinheim, 2004.	0
D. A. Skoog, D. M. West i F. J. Holler, S. R. Crouch, Fundamentals of Analytical Chemistry, 9th edition, Brooks&Cole, SAD, 2014.	0

Optional literature (at the time of submission of study programme proposal)

Z. Šoljić, Računanje u analitičkoj kemiji, Zagreb, 1998.

Quality assurance methods that ensure the acquisition of exit competences

- Monitoring suggestions and reactions of students during the semester
- Student survey

Other (as the proposer wishes to add)