Exercises in Instrumental Methods of Analysis

NAME OF THE COURSE Exercises in Instrumental Methods of Analysis

Code

KTG303

Year of study

3.

Course teacher

Asst Prof Lea Kukoč Modun

Credits (ECTS)

2.0

Associate teachers

Maja Biočić
Andrea Anđić
Azra Đulović

Type of instruction (number of hours)

P S V T

0

0

30

0

Status of the course

Mandatory

Percentage of application of e-learning

0 %

COURSE DESCRIPTION

Course objectives

After completion of a process of learning the learner is able for independent work in instrumental analytical laboratory

Course enrolment requirements and entry competences required for the course

Enrolled in or passed the course Instrumental Methods of Analysis

Learning outcomes expected at the level of the course (4 to 10 learning outcomes)

1. Adopt theoretical knowledge related to methods of instrumental analysis (spectrometry , electroanalytical , thermal methods , instrumental methods for separation ) and principles of instruments and apply knowledge in the experimental work.
2. Select analytical technique due to the characteristics of the analyte and the specificity of the sample.
3. Plan and install an experiment using instrumental techniques.
4. Apply basic statistical analysis of numerical data and graphed the results.
5. Independently take Lab Notes and prepare a report after completion of the analysis.

Course content broken down in detail by weekly class schedule (syllabus)

1. Kinetic methods of analysis, determoination of tiolic compound using kinetic manifold with spectrophotometric detector
2. Flow injection analysis, determination of ascorbic acid by flow injection analysis and spectrophotometric detector
3. UV/Vis spectrophotometry, spectrophotometric measurement of an equilibrium constant
4. Atomic absorption spectroscopy, determination of metals in real samples
5. Ions selective electrode, potentiometry, measurement of an equilibrium constant
6. Electrogravimetric determination, determination or separation of metals

Format of instruction:

Student responsibilities

Students must attend classes regularly and do all laboratory exercises in planned
program.

Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course):

Class attendance

0.0

Research

0.0

Practical training

0.0

Experimental work

0.8

Report

0.4

 

 

Essay

0.0

Seminar essay

0.0

 

 

Tests

0.8

Oral exam

0.0

 

 

Written exam

0.0

Project

0.0

 

 

Grading and evaluating student work in class and at the final exam

The rating is formed from three parts: tests which is 40 % of the grade , the experimental section, which is 40 % of the grade , and Report, which is the remaining 20 % of the grade.

Required literature (available in the library and via other media)

Title

Number of copies in the library

Availability via other media

D.A. Skoog, D.M. West, F.J. Holler, Osnove analitičke kemije, šesto izdanje (englesko), prvo izdanje (hrvatsko), Školska knjiga, Zagreb, 1999.

18

I. S. Krull, Analytical Chemistry, Intech, Rijeka, 2012.

0

dostupno na webu: DOI: 10.5772/3086

L. Kukoč, Molekulska spektroskopija, Interna recenirana skripta, 2003.

30

dostupno u digitalnom obliku

L. Kukoč, Spektrometrijske metode elementne analize, Interna recenirana skripta, 2005.

30

dostupno u digitalnom obliku

Josipa Komljenović, Ion selektivna sulfidna elektroda, Interna recenzirana skripta

30

dostupno u digitalnom obliku

Optional literature (at the time of submission of study programme proposal)

Nj. Radić i L. Kukoč Modun, Uvod u analitičku kemiju I. dio, Redak, Split, 2013.
R. Kellner, J. M. Mermet, M. Otto, M. Valcarcel and H. M. Widmer (Urednici), Analytical Chemistry (A Modern Approach to Analytical Science, Second Edition) Wiley-VCHVerlag Gmbh & Co. KGaA, Weinheim, 2004.
D. A. Skoog, D. M. West, F. J. Holler and S. R. Crouch, Fundamentals of Analytical Chemistry, Eighth Edition, Thompson Brooks/Cole, Belmont, USA, 2004.
D. Harvey, Modern Analytical Chemistry, McGraw-Hill Higher Education, New York, London, 2000.
F. W. Fifield & D. Kealey, Principles and Practice of Analytical Chemistry, Blackwell Science Ltd, Malde

Quality assurance methods that ensure the acquisition of exit competences

Quality assurance will be performed at three levels:
(1) University Level; (2) Faculty Level by Quality Control Committee; (3) Lecturer’s Level.

Other (as the proposer wishes to add)