Physical methods of analysis

Code

Course teacher

Associate teachers

Status of the course

Course objectives

Acquisition of basic knowledge about the physical methods of analysis based on optical and electrochemical phenomena. To enable students to understand and apply the acquired knowledge in practice in the analysis of complex samples

Course enrolment requirements and entry competences required for the course

Completed appropriate undergraduate study

Learning outcomes expected at the level of the course (4 to 10 learning outcomes)

1. Adoption of the basic knowledge and principles of the application of spectroscopic techniques for analysis of complex samples
2. Understand and apply the methods of sample preparation for chemical analysis
3. Apply spectroscopic analysis methods in the analysis of complex samples.
4. Implement separation analysis methods in the analysis of complex samples.
5. Apply the principles of validation of the analytical method

Course content broken down in detail by weekly class schedule (syllabus)

1. week: Analytical system. Sampling from the environment. Seminar: Solving problems.
2. Week: Preparation of the sample for analysis. Seminar: Solving problems.
3. week: Method of isolation of the analyte from the nuts: solid phase extraction, microwave ultrasonic extraction. Seminar: Solving problems.
4. Week: Spectroscopic methods. Molecular Spectroscopy. Seminar: Solving problems.
5. Week: Atomic absorption spectroscopy, mass spectroscopy. Seminar: Solving problems.
6. week: Chromatographic methods: gas, ion, thin layer chromatography. Seminar: Solving problems.
7. Week : 1st. partial exam, solving the test
8. week: High performance liquid chromatography. Seminar: Solving problems.
9. week: Validation of methods. Comparison of methods. The choice of the appropriate method. Seminar: Solving problems
10. Week: Statistical analysis and evaluation of results, and obtain information about the sample. Seminar: Solving problems
11. Week: Validation of spectoscopic methods, examples. Seminar: Solving problems
12.Validation of chromatographic methods examples. Seminar: Solving problems
13 Week: Automation in the analytical laboratory. Segmented flow method. Seminar: Solving problems
14. Week: flow-injection method. An automated analytical systems. Seminar: Solving problems
15. Week : 2 nd partial exam , solving the test

Format of instruction:

Student responsibilities

Lectures attendance - at least 80% and completing exercises