NAME OF THE COURSE |
Physical methods of analysis |
Code |
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Course teacher |
Prof Josipa Giljanović |
Credits (ECTS) |
6.0 |
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Associate teachers |
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Type of instruction (number of hours) |
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Status of the course |
Elective |
Percentage of application of e-learning |
0 % |
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COURSE DESCRIPTION |
Course objectives |
Acquisition of basic knowledge about the physical methods of analysis based on optical and electrochemical phenomena. To enable students to understand and apply the acquired knowledge in practice in the analysis of complex samples |
Course enrolment requirements and entry competences required for the course |
Completed appropriate undergraduate study |
Learning outcomes expected at the level of the course (4 to 10 learning outcomes) |
1. Adoption of the basic knowledge and principles of the application of spectroscopic techniques for analysis of complex samples 2. Understand and apply the methods of sample preparation for chemical analysis 3. Apply spectroscopic analysis methods in the analysis of complex samples. 4. Implement separation analysis methods in the analysis of complex samples. 5. Apply the principles of validation of the analytical method |
Course content broken down in detail by weekly class schedule (syllabus) |
1. week: Analytical system. Sampling from the environment. Seminar: Solving problems. 2. Week: Preparation of the sample for analysis. Seminar: Solving problems. 3. week: Method of isolation of the analyte from the nuts: solid phase extraction, microwave ultrasonic extraction. Seminar: Solving problems. 4. Week: Spectroscopic methods. Molecular Spectroscopy. Seminar: Solving problems. 5. Week: Atomic absorption spectroscopy, mass spectroscopy. Seminar: Solving problems. 6. week: Chromatographic methods: gas, ion, thin layer chromatography. Seminar: Solving problems. 7. Week : 1st. partial exam, solving the test 8. week: High performance liquid chromatography. Seminar: Solving problems. 9. week: Validation of methods. Comparison of methods. The choice of the appropriate method. Seminar: Solving problems 10. Week: Statistical analysis and evaluation of results, and obtain information about the sample. Seminar: Solving problems 11. Week: Validation of spectoscopic methods, examples. Seminar: Solving problems 12.Validation of chromatographic methods examples. Seminar: Solving problems 13 Week: Automation in the analytical laboratory. Segmented flow method. Seminar: Solving problems 14. Week: flow-injection method. An automated analytical systems. Seminar: Solving problems 15. Week : 2 nd partial exam , solving the test |
Format of instruction: |
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Student responsibilities |
Lectures attendance - at least 80% and completing exercises |
Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course): |
Class attendance |
0.5 |
Research |
0.0 |
Practical training |
2.5 |
Experimental work |
0.0 |
Report |
0.0 |
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Essay |
0.0 |
Seminar essay |
1.5 |
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Tests |
0.0 |
Oral exam |
1.0 |
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Written exam |
1.0 |
Project |
1.0 |
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Grading and evaluating student work in class and at the final exam |
The entire test can be applied over two partial tests during the semester. Passing threshold is 60%. Each test in assessing participates with 50%. Lectures presence of 80 to 100% is 10% marks. The examination periods there is a written and oral exam. Passing threshold is 60%. Passing one partial test of any part (previous activity) is valid throughout current academic year. Written exam has a share of 50% and oral examination also 50%. Students who have not passed the partial tests will have oral examination in the regular examination period. Passing threshold is 60% and the examination form to participate in the evaluation by 50%. Rating: 60% -69% - satisfactory, 70% -79% - good, 80% -89% very good, 90% -100% - excellent. |
Required literature (available in the library and via other media) |
Title |
Number of copies in the library |
Availability via other media |
D. A.Skoog, D. M. West, F. J. Holler, Fundamentals of Analytical Chemistry, Seventh Edition, Saunders College Publishing, New York, London, 1996. { šesto izdanje (englesko) 1992, prvo izdanje (hrvatsko), Školska knjiga, Zagreb, 1999.}; |
6 |
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A. Skoog, D. M. West i F. J. Holler, S. R. Crouch, Fundamentals of Analytical Chemistry, 9th edition, Brooks&Cole, SAD, 2014.; 3.D.C.Harris, Quantitative Chemical Analysis, Eighth Edition, W.H.Freeman and Company, New York, 2010. |
0 |
na web-stranici Zavoda za analitičku kemiju |
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Optional literature (at the time of submission of study programme proposal) |
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Quality assurance methods that ensure the acquisition of exit competences |
- registration of student’s presence in class - annual analysis of students success in this course - student’s survey in order to evaluate the professor - professor’s self-evaluation |
Other (as the proposer wishes to add) |
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