Exercises in Analytical Chemistry II

NAME OF THE COURSE

Code

KTG204

Year of study

Course teacher

Assoc Prof Lea Kukoč Modun

Credits (ECTS)

4.0

Associate teachers

ScD Maja Biočić

Type of instruction (number of hours)

P	S	V	T
0	0	60	0

Status of the course

Mandatory

Percentage of application of e-learning

0 %

COURSE DESCRIPTION

Course objectives

Students gain basic knowledge of working in the analytical laboratory, the proper approach to chemical analysis of samples, the possibility of critical reasoning based on knowledge, the chemical changes in the experimental work , correct writing lab reports in accordance with good laboratory practices.

Course enrolment requirements and entry competences required for the course

Enrolled in or passed the course Analytical Chemistry II

Learning outcomes expected at the level of the course (4 to 10 learning outcomes)

1. Apply standard laboratory procedures in gravimetric analysis.
2. Apply titration based on homogenous or heterogeneous equilibrium with previous theoretical predictions.
4. Apply the principles of good laboratory practice.
5. Properly collect and process numerical data.
6. Write the appropriate laboratory report.

Course content broken down in detail by weekly class schedule (syllabus)

1. (6 hours) Determinations based on heterogeneous equilibrium. Argentometric titration.
2. (6 hours) Potentiometric titration.
3. (6 hours) Gravimetric determination of sulphate ion.
4. (6 hours) Gravimetric determination of nickel ion.
5. (4 hours) Preparing standard solution, acid-base titration.
6. (6 hours) Acid-base titration, determination of H2C2O4.
7. (6 hours) Finding the end point with pH electrode.
8. (4 hours) Preparing standard solution, EDTA titration.
9. (6 hours) EDTA titration, determination of Fe3+.
10. (4 hours) Preparing standard solution, redox titration.
11. (6 hours) Redox titration, determination of Cu2+.

Format of instruction:

Student responsibilities

Students must attend classes regularly and do all laboratory exercises in planned program.

Screening student work (name the proportion of ECTS credits for eachactivity so that the total number of ECTS credits is equal to the ECTS value of the course):

Class attendance	0.0	Research	Practical training	1.6
Experimental work	0.0	Report		0.8
Essay	0.0	Seminar essay
Tests	1.6	Oral exam
Written exam	0.0	Project

Grading and evaluating student work in class and at the final exam

The rating is formed from three parts: tests which is 40 % of the grade , the experimental section, which is 40 % of the grade , and Lab Notebook, which is the remaining 20 % of the grade.

Required literature (available in the library and via other media)

Title	Number of copies in the library	Availability via other media
A. Prkić, Vježbe iz analitičke kemije, Preddiplomski studij kemijske tehnologije, interna recenzirana skripta, Split, 2008. (odabrana poglavlja)	0	dostupno u digitalnom obliku
Vježbe iz kvalitativne analitičke kemije, dr. sc. Josipa Komljenović, doc. (odabrana poglavlja)	0	dostupno

Optional literature (at the time of submission of study programme proposal)

1. D.A. Skoog, D.M. West, F.J. Holler, Osnove analitičke kemije, šesto izdanje (englesko), prvo izdanje (hrvatsko), Školska knjiga, Zagreb, 1999.
2. Nj. Radić i L. Kukoč Modun, Uvod u analitičku kemiju, Zagreb, 2016.
3. Nj. Radić i L. Kukoč Modun, Uvod u analitičku kemiju I. dio, Redak, Split, 2013..
4. M. Kaštelan-Macan, Kemijska analiza u sustavu kvalitete, Školska knjiga, Zagreb 2003.

Quality assurance methods that ensure the acquisition of exit competences

Quality assurance will be performed at three levels:
(1) University Level; (2) Faculty Level by Quality Control Committee; (3) Lecturer’s Level.

Other (as the proposer wishes to add)